Analysis of methods for studying the size of nanoparticles
G.I. Sverdlik, A.Yu. Ataeva, A.R. Ataev, E.A. Khadzaragova, L.T. Vazieva
North Caucasian Institute of Mining and Metallurgy (State Technological University)
DOI: 10.26456/pcascnn/2021.13.358
Original article
Abstract: In the presented work, various methods for determining the size of nanoparticles are considered. An effective method for finding possible options has been determined. Information on various methods and studies was selected and analyzed. Fundamentally different methods for finding the sizes of nanoparticles are considered. Non-contact (optical) methods are the most promising. The particle size ranges of the investigated particles are analyzed and presented using the next methods: optical microscopy, electron microscopy, scanning probe microscopy. The principles of operation and possible schemes of installations for studying the material under study are described. The sedimentation method, using centrifugation and the X-ray principle of detection, is described in more detail. Its advantages over other methods are noted. Examples are given of its use in an experimental setup that allows obtaining differential and integral characteristics in various bases, which make it possible to analyze the particle size distribution in the granulometric study of materials, including nanomaterials.
Keywords: nanoparticles, sedimentation method, sedimentometer, gravity sedimentation, centrifugation, differential and integral curves
- Grigorii I. Sverdlik – Dr. Sc., Professor of the Department «Technological Machines and Equipment», North Caucasian Institute of Mining and Metallurgy (State Technological University)
- Angela Yu. Ataeva – Ph.D., Docent, Department «Technological Machines and Equipment», Director of the Center of Collective Use of Scientific Equipment, North Caucasian Institute of Mining and Metallurgy (State Technological University)
- Amond R. Ataev – Master's degree, Faculty of Architecture and Civil Engineering, North Caucasian Institute of Mining and Metallurgy (State Technological University)
- Elena A. Khadzaragova – Dr. Sc., Professor, Vice-Rector for Research and Innovation, North Caucasian Institute of Mining and Metallurgy (State Technological University)
- Lyudmila T. Vazieva – Ph.D., Docent, Head of the Department «Physical and Mathematical Disciplines», North Caucasian Institute of Mining and Metallurgy (State Technological University)
Reference:
Sverdlik, G.I. Analysis of methods for studying the size of nanoparticles / G.I. Sverdlik, A.Yu. Ataeva, A.R. Ataev, E.A. Khadzaragova, L.T. Vazieva // Physical and chemical aspects of the study of clusters, nanostructures and nanomaterials. — 2021. — I. 13. — P. 358-367. DOI: 10.26456/pcascnn/2021.13.358. (In Russian).
Full article (in Russian): download PDF file
References:
1. Sverdlik G.I., Vyskrebenets A.S., Ataeva A.Yu. Raspredelitel'naya tarelka massoobmennogo apparata dlya mokroi ochistki gaza [Distribution tray of mass transfer apparatus for wet gas cleaning]. Patent RF, no. 2303479, 2007. (In Russian).
2. Sverdlik G.I., Vickrebenets A.S., Maxsimov R.N., Ataeva A.Y. Issledovanie parametrov dlya polucheniya pennogo rezhima v strujnom barbotere [Research of parameters of a foam in the jet regime bubbler], Fiziko- khimicheskie aspekty izucheniya klasterov, nanostruktur i nanomaterialov [Physical and chemical aspects of the study of clusters, nanostructures and nanomaterials], 2017, issue 9, pp. 430-434. DOI: 10.26456/pcascnn/2017.9.430. (In Russian).
3. Krushenko G.G., Reshetnikova S.N Problemy opredeleniya razmerov nanochastits [Detecting sizes of of chemical compounds nanoparticles], Tekhnologicheskie problemy i materialy. Vestnik SibGAU [Bulletin of the Siberian state aerospace university after ACADEMIC M.F. Reshetnev], 2011, no. 2, pp. 167-170. (In Russian).
4. Clarke A., Eberhardt C. Microscopy techniques for materials science. Boca Raton, CRC Press; Cambridge, Woodhead Publ., 2002, 456 p.
5. Shindo D., Oikawa T. Analytical electron microscopy for materials science. Tokyo, Springer, 2002, ix, 152 p. DOI: 10.1007/978-4-431-66988-3.
6. Shabanova N.A., Popov V.V., Sarkisov P.D. Chemistry and technology of nanodispersed oxides [Khimiya i tekhnologiya nanodispersnykh oksidov]. Moscow IKTS Akademkniga Publ., 2006, 310 p. (In Russian).
7. Ataeva A.Yu., Sverdlik G.I., Kambolov D.A., Ataev A.R. Sovremenyye metody granulometricheskogo analiza pylevidnykh materialov, soderzhashchikh nanochastitsy [Modern methods of granulometric analysis of dusted materials containing nanoparticles], Fiziko-khimicheskie aspekty izucheniya klasterov, nanostruktur i nanomaterialov [Physical and chemical aspects of the study of clusters, nanostructures and nanomaterials], 2020, issue 12, pp. 706-712. DOI: 10.26456/pcascnn/2018.10.044. (In Russian).
8. Temam R. Navier–Stokes equations: theory and numerical analysis. Bloomington, Indiana University, AMS Chelsea Publishing, 1984, vol. 343, 408 p. DOI: 10.1090/chel/343.
9. Hann D.B., Cherdantsev A.V., Azzopard B.J. Study of bubbles entrapped into a gas-sheared liquid film, International Journal of Multiphase Flow, 2018, vol. 108, pp. 181-201. DOI: 10.1016/j.ijmultiphaseflow.2018.07.001.
10. Xiao H., Geng S., Chen A. et al. Bubble formation in continuous liquid phase under industrial jetting conditions, Chemical Engineering Science, 2019, vol. 200, pp. 214-224. DOI: 10.1016/j.ces.2019.02.009.