Physical and chemical aspects of the study of clusters, nanostructures and nanomaterials. Founded at 2009

INFLUENCE OF CALCINATION TEMPERATURE ON STRUCTURAL CHANGES OF NANOSIZED ZIRCONIA

D.G. Selemeneva, A.A. Kravtsov, A.V. Blinov, M.A. Jasnaja

DOI: 10.26456/pcascnn/2015.7.450

Original article

Abstract: The synthesis of nanosized zirconia by sol-gel method was performed. The optimal conditions for stable ZrO2 gel was determined, and then was set a point of gelation. Obtained samples of zirconia nanoparticles were studied by infrared spectroscopy and XRD analysis. Acid-base properties of the surface of the samples were studied by indicator method.

Keywords: sol-gel method, ZrO2 nanoparticles, infrared spectroscopy, X-ray difraction analysis, indicator method

  • D.G. Selemeneva
  • A.A. Kravtsov
  • A.V. Blinov
  • M.A. Jasnaja

Reference:

Selemeneva D.G., Kravtsov A.A., Blinov A.V., Jasnaja M.A. Vliyanie temperatury prokalivaniya na strukturnye izmeneniya nanorazmernogo dioksida tsirkoniya [INFLUENCE OF CALCINATION TEMPERATURE ON STRUCTURAL CHANGES OF NANOSIZED ZIRCONIA], Fiziko-khimicheskie aspekty izucheniya klasterov, nanostruktur i nanomaterialov [Physical and chemical aspects of the study of clusters, nanostructures and nanomaterials], 2015, issue 7, pp. 450-455. DOI: 10.26456/pcascnn/2015.7.450. ⎘

Full article (in Russian): download PDF file

Content |