INFLUENCE OF CALCINATION TEMPERATURE ON STRUCTURAL CHANGES OF NANOSIZED ZIRCONIA
D.G. Selemeneva, A.A. Kravtsov, A.V. Blinov, M.A. Jasnaja
DOI: 10.26456/pcascnn/2015.7.450
Original article
Abstract: The synthesis of nanosized zirconia by sol-gel method was performed. The optimal conditions for stable ZrO2 gel was determined, and then was set a point of gelation. Obtained samples of zirconia nanoparticles were studied by infrared spectroscopy and XRD analysis. Acid-base properties of the surface of the samples were studied by indicator method.
Keywords: sol-gel method, ZrO2 nanoparticles, infrared spectroscopy, X-ray difraction analysis, indicator method
- D.G. Selemeneva
- A.A. Kravtsov
- A.V. Blinov
- M.A. Jasnaja
Reference:
Selemeneva, D.G. INFLUENCE OF CALCINATION TEMPERATURE ON STRUCTURAL CHANGES OF NANOSIZED ZIRCONIA / D.G. Selemeneva, A.A. Kravtsov, A.V. Blinov, M.A. Jasnaja // Physical and chemical aspects of the study of clusters, nanostructures and nanomaterials. — 2015. — I. 7. — P. 450-455. DOI: 10.26456/pcascnn/2015.7.450. (In Russian).
Full article (in Russian): download PDF file
Content |